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Detection and imaging of reactive oxygen species associated with the electrochemical oxygen evolution by hydrodynamic scanning electrochemical microscopy

Iffelsberger, Christian ; Raith, Timo ; Vatsyayan, Preety ; Vyskočil, Vlastimil ; Matysik, Frank-Michael


Hydrodynamic scanning electrochemical microscopy (SECM) was applied for the characterization of Pt and boron-doped diamond (BDD) macroelectrodes operated in a potential region producing reactive oxygen species (ROS) during oxygen evolution reaction (OER). Forced convection introduced by high-precision stirring enabled the formation of a stable diffusion layer of electrochemically produced species ...


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