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Bile acids: Electrochemical oxidation on bare electrodes after acid-induced dehydration

Klouda, Jan ; Barek, Jiří ; Kočovský, Pavel ; Herl, Thomas ; Matysik, Frank-Michael ; Nesměrák, Karel ; Schwarzová-Pecková, Karolina


Bile acids and sterols in general have long been considered practically inactive for direct redox processes. Herein, a novel way of electrochemical oxidation of primary bile acids is reported, involving an initial acid-induced dehydration step, as confirmed by capillary electrophoresis-mass spectrometry, thereby extending the electrochemical activity of the steroid core. Oxidation potentials were ...


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