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Direct C–H Bond Imidation with Benzoyl Peroxide as a Mild Oxidant and a Reagent

Brandhofer, Tobias ; Gini, Andrea ; Stockerl, Sebastian ; Piekarski, Dariusz G. ; García Mancheño, Olga


A simple and mild Cu-catalyzed oxidative three component oxidative Ugi-type method for the synthesis of a variety of substituted imides has been developed. In this direct imidation approach, benzoyl peroxide serves as both the oxidant and the carboxylate source, allowing not only the functionalization of C(sp(3))-H bonds in alpha-position to an amine but also benzylic substrates. This procedure ...


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