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Monitoring Dynamics, Structure, and Magnetism of Switchable Metal–Organic Frameworks via 1 H‐Detected MAS NMR

URN to cite this document:
urn:nbn:de:bvb:355-epub-492509
DOI to cite this document:
10.5283/epub.49250
Blahut, Jan ; Lejeune, Arthur L. ; Ehrling, Sebastian ; Senkovska, Irena ; Kaskel, Stefan ; Wisser, Florian M. ; Pintacuda, Guido
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Date of publication of this fulltext: 09 Sep 2021 04:49


Abstract

We present a toolbox for the rapid characterisation of powdered samples of paramagnetic metal–organic frameworks at natural abundance by 1H-detected solid-state NMR. Very fast MAS rates at room and cryogenic temperatures and a set of tailored radiofrequency irradiation schemes help overcome the sensitivity and resolution limits often associated with the characterisation of MOF materials. We ...

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