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Nickel-catalyzed and Li-mediated regiospecific C–H arylation of benzothiophenes

Mohr, Yorck ; Hisler, Gaëlle ; Grousset, Léonie ; Roux, Yoann ; Quadrelli, Elsje Alessandra ; Wisser, Florian M. ; Canivet, Jérôme



Abstract

A nickel-based catalytic system for the regiospecific C2-H arylation of benzothiophene has been established. NiCl2(bpy) is used as a catalyst in combination with LiHMDS as a base in dioxane. The catalytic system is applicable to a variety of functionalized benzothiophenes, as well as other heteroarenes including thiophene, benzodithiophene, benzofuran and selenophene in combination with iodo aryl ...

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