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Lanthanide orthothiophosphates revisited: single-crystal X-ray, Raman, and DFT studies of TmPS4 and YbPS4

Scholz, Tanja ; Pielnhofer, Florian ; Eger, Roland ; Lotsch, Bettina V.



Zusammenfassung

The crystal structures of the lanthanide orthothiophosphates LnPS(4) (Ln = lanthanide) have been extensively investigated in the past. Up to now, however, single crystals of two members of this series - TmPS4 and YbPS4 - have not been available. Here, we report a modified synthesis protocol for TmPS4 and YbPS4 yielding single crystals suitable for X-ray diffraction. Both compounds crystallize in ...

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