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Towards a General Access to 1-Azaspirocyclic Systems via Photoinduced, Reductive Decarboxylative Radical Cyclizations

Kiprova, Natalia ; Desnoyers, Marine ; Narobe, Rok ; Klufts-Edel, Arthur ; Chaud, Juliane ; König, Burkhard ; Compain, Philippe ; Kern, Nicolas


A convenient and versatile approach to important 1-azaspirocyclic systems relevant to medicinal chemistry and natural products is reported herein. The main strategy relies on a reductive decarboxylative cyclization of redox-active esters which can be rapidly assembled from abundant cyclic azaacids and tailored acceptor sidechains, with a focus on alkyne acceptors enabling the generation of useful ...


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