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Photo‐Induced Homologation of Carbonyl Compounds for Iterative Syntheses

Wang, Hua ; Wang, Shun ; George, Vincent ; Llorente, Galder ; König, Burkhard
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We describe a photo-induced reaction for the in situ generation of highly reactive alkyl diazo species from carbonyl precursors via photo-excitation of N-tosylhydrazone anions. The diazo intermediates undergo efficient C-H insertion of aldehydes, leading to the productive synthesis of aldehydes and ketones. The method is applicable to the iterative synthesis of densely functionalized carbonyl ...


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