Abstract
The ammonolysis of SiS2 in liquid ammonia yields crystalline (NH4)(2)[SiS3(NH3)]center dot 2NH(3), which contains [SiS3(NH3)] (2-) as a derivative of the ortho-thiosilicate anion SiS44-.
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The first thiosilicate from solution: synthesis and crystal structure of (NH4)2[SiS3(NH3)]·2NH3
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