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Synthesis of a bicyclic diamine derived from Kemp´s acid

Schmaderer, Harald ; Hohenleutner, Andreas ; König, Burkhard



Abstract

A bicyclic diamine with defined and stable conformation in solution
was prepared from Kemp’s triacid. The efficient four-step synthesis of the Boc-protected diamine requires only a single purification by column chromatography. X-ray analysis and NMR spectroscopy confirm the structure of the diamine in the solid state and in solution.


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