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Gs-HSQC-NOESY versus gs-NOESY-HSQC experiments: Signal attenuation due to diffusion; application to symmetrical molecules

Gschwind, R. M. ; Xie, X. ; Rajamohanan, P. R.



Abstract

Gradient-selected (gs) HSQC-NOESY type experiments are often applied in order to obtain NOE cross peaks in symmetrical molecules or in complex organic molecules, e.g. carbohydrates. Since the coherence-selecting gradients in these pulse sequences are separated by several delays, including the mixing time, the gs-HSQC-NOESY spectra exhibit severe signal attenuation due to diffusion effects. The ...

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