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O-silylierter Milchaldehyd - Diastereomere Derivate
Tanner, U., Eibler, E., Burgemeister, T. and Wiegrebe, Wolfgang (1992) O-silylierter Milchaldehyd - Diastereomere Derivate. Pharmazeutische Zeitung 137, pp. 78-83.Date of publication of this fulltext: 12 Jul 2010 05:17
Article
DOI to cite this document: 10.5283/epub.15742
Abstract
The title compound 2 was obtained either by reduction of O-silylated methyl lactate (1) with diisobutylaluminiumhydrid or by Os04-degradation of the allyl alcohol 5.2 was converted to diastereomeric derivatives, inter alia 7 and 9, suitable for 1H-NMR- or HPLC-determination of the absolute configuration of minor amounts of 2. Die Titelverbindung 2 wurde entweder aus dem ...
The title compound 2 was obtained either by reduction of O-silylated
methyl lactate (1) with diisobutylaluminiumhydrid
or by Os04-degradation of the allyl alcohol 5.2 was converted
to diastereomeric derivatives, inter alia 7 and 9, suitable for
1H-NMR- or HPLC-determination of the absolute configuration
of minor amounts of 2.
Die Titelverbindung 2 wurde entweder aus dem O-silylierten
Milchsäureester 1 durch Reduktion mit Diisobutylaluminiumhydrid
oder durch Os04-Abbau des Allylalkohols 5
erhalten. 2 wurde in diastereomere Derivate, u. a. 7 und 9,
überführt, die sich zur Bestimmung der absoluten Konfiguration
kleiner Mengen von 2 eignen.
Involved Institutions
Details
| Item type | Article |
| Journal or Publication Title | Pharmazeutische Zeitung |
| Volume: | 137 |
|---|---|
| Page Range: | pp. 78-83 |
| Date | 1992 |
| Institutions | Chemistry and Pharmacy > Institute of Pharmacy > Alumni or Retired Professors > Prof. Wiegrebe |
| Dewey Decimal Classification | 500 Science > 540 Chemistry & allied sciences |
| Status | Published |
| Refereed | Yes, this version has been refereed |
| Created at the University of Regensburg | Unknown |
| URN of the UB Regensburg | urn:nbn:de:bvb:355-epub-157422 |
| Item ID | 15742 |
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