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O-silylierter Milchaldehyd - Diastereomere Derivate

URN to cite this document:
urn:nbn:de:bvb:355-epub-157422
Tanner, U. ; Eibler, E. ; Burgemeister, T. ; Wiegrebe, Wolfgang
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Date of publication of this fulltext: 12 Jul 2010 05:17


Abstract

The title compound 2 was obtained either by reduction of O-silylated methyl lactate (1) with diisobutylaluminiumhydrid or by Os04-degradation of the allyl alcohol 5.2 was converted to diastereomeric derivatives, inter alia 7 and 9, suitable for 1H-NMR- or HPLC-determination of the absolute configuration of minor amounts of 2. Die Titelverbindung 2 wurde entweder aus dem ...

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