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Crystal Structure of (-)-Corycavinium(+)-10-Camphorsulfonate, a Biosynthetic Intermediate to Hexahydrobenzo[c]phenanthridine Alkaloids

URN to cite this document:
urn:nbn:de:bvb:355-epub-157854
Kamigauchi, M. ; Noda, Y. ; Iwasa, K. ; Nishijo, Z. ; Ishida, T. ; In, Y. ; Wiegrebe, Wolfgang
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Date of publication of this fulltext: 12 Jul 2010 09:41


Abstract

The crystal structure of (—)-corycavinium (+)-10-camphorsulfonate has been investigated by X-ray analysis. The structure of (-)-corycavinium ion ( = (-)-(7S,13S,14R)-5,6,13,13a-tetrahydro-l3a-hydroxy-7-methyl- 2,3;9,10-bis(methylenedioxy)-8H-dibenzo[a,g]quinolizinium), has been determined. The conformation with B/Ccis -conjunction, a twisted half-chair of ring B, and a half-chair of ring C, as ...

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