Synthesis, spectroscopic investigation and molecular structure of pentacarbonyl-5-t-butyl-5-aza-2,8-dithia-1-stannobicyclo[3.3.01,5]octanechromium(0)

Tzschach, A., Jurkschat, K., Scheer, Manfred, Meunier-Piret, J. und Meerssche, M. van (1983) Synthesis, spectroscopic investigation and molecular structure of pentacarbonyl-5-t-butyl-5-aza-2,8-dithia-1-stannobicyclo[3.3.01,5]octanechromium(0). Journal of Organometallic Chemistry 259 (2), S. 165-170.

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Zusammenfassung

The compound pentacarbonyl-5-t-butyl-5-aza-2,8-dithia-1-stannobicyclo-[3.3.01,5]octanechromium(0) was prepared in good yield by the reaction of 5-t-butyl-5-aza-2,8-dithia-1-stannobicyclo[3.3.01,5]octane with Cr(CO)6 in THF under UV-irradiation. The crystal and molecular structure was determined from three-dimensional X-ray data. The crystals are monoclinic, space group P21/c. The unit cell, with ...

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