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The structure of 5-aza-2,8-dioxa-1-stanna(II)bicyclo[3.3.0]octane

DOI to cite this document:
10.5283/epub.16004
Zschunke, A. ; Mügge, C. ; Scheer, Manfred ; Jurkschat, K. ; Tzschach, A.
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Date of publication of this fulltext: 26 Jul 2010 11:20


Abstract

From the1H,13C, and119Sn NMR spectra at different temperatures, it is concluded that the 5-alkyl-5-aza-2,8-dioxa-1-stanna(II)bicyclo[3.3.0]octanes dimerize in nonpolar solvents. The barrier for dimerization is lower (G =40 kJ/mol) than the barrier for simultaneous dissociation-inversion (G =70 kJ/mol). The dimers studied are sterically uniform.


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