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Tumor inhibiting properties of stereoisomeric [1,2-bis(3-hydroxyphenyl)ethylenediamine]dichloroplatinum(II) complexes. Part I. Synthesis

Jennerwein, Margaretha ; Gust, Ronald ; Müller, Richard ; Schönenberger, Helmut ; Engel, Juergen ; Berger, Martin R. ; Schmaehl, Dietrich ; Seeber, Siegfried ; Osieka, Reinhardt



Abstract

The prepn. of stereoisomeric 1,2-bis(3-hydroxyphenyl)ethylenediamines (L) from meso-1,2-bis(2-hydroxyphenyl)ethylenediamine and 3-methoxybenzaldehyde by a diaza-Cope-rearrangement and subsequent ether cleavage with BBr3 and their conversion to PtLCl2 with K2PtCl4 are described. PtLCl2 were characterized by CD, IR and NMR spectra.


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