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Protonenresonanz-Untersuchungen zur inneren Rotation 6: The conformers of a nitrosamine and a carboxamide: Comparison of NMR line shape and equilibration methods

Jaeschke, A. ; Münsch, Helmut ; Schmid, H. G. ; Friebolin, H. ; Mannschreck, Albrecht


Activation parameters for the interconversion of conformers IA and IB of neopentylbenzylnitrosamine and of rotamers IIA and IIB of N,2,4,6-tetramethyl-N-benzylbenzamide were determined by two techniques: Equilibration of pure IB (or IIA, respectively) and subsequent measurement of 1H-NMR line shapes with the same sample. Ea- and k0-values obtained by the two methods agree well within error ...


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