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Antimycotics. III. Comparative studies of the preparation of isomeric hydroxybenzamides

Schönenberger, Helmut ; Holzheu-Eckardt, Juergen ; Bamann, Eugen



Abstract

cf. CA 60, 16248e. HOC6H4CONHR (I), active antimycotics (CA 59, 2070e), were prepd. by SOCl2 treatment of HOC6H4CO2H (II), MeOC6H4CO2H (III), AcOC6H4CO2H (IV), or MeO2COC6H4CO2H (V) and aminolysis of the resulting HOC6H4COCl (VI), MeOC6H4COCl (VII), AcOC6H4COCl (VIII), or MeO2COC6H4COCl (IX), followed by hydrolytic removal of the protecting Ac and MeO2C groups in AcOC6H4CONHR (X) and ...

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