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Alkoxybenzhydrylalkylamines and their acid addition salts

Thies, Heinrich ; Schönenberger, Helmut



Abstract

The title amines (I) are prepd. by reaction of the corresponding alkoxybenzylidenealkylamine (II) with PhLi followed by hydrolysis. Thus, 32 g. PhBr was added dropwise to 2.8 g. Li wire in 100 ml. dry Et2O under N. To the product was added 11.3 g. 4-methoxybenzylidenepropylamine in 30 ml. Et2O and the mixt. shaken for 2 hrs. to give 82.6% I (R = 4-MeO, R1 = Pr), b12 199-202 Deg; hydrochloride m. ...

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