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Anwendung der NMR-Spektroskopie chiraler Assoziate 8: rotation about the C(sp²)—C(aryl) bond in 2,6-disubstituted Benzamides

Holík, M. ; Mannschreck, Albrecht



Abstract

The barrier to rotation about the C(sp2)C(aryl) single bond in non-planar benzoyl compounds was investigated using N,N-dimethyl, N,N-tetramethylene and N,N-diisopropyl derivatives of 2,4,6-trimethylbenzamide and 2,6-dimethoxybenzamide and N,N-dimethyl derivatives of the corresponding thiobenzamides. Their 1H and 13C NMR spectra were determined and assigned and the splittings in the 1H spectra due ...

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