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Flüssigkeits-Chromatographie an Triacetylcellulose 7: Characterization of a sorbent for the separation of enantiomers

Koller, H. ; Rimböck, Karl-Heinz ; Mannschreck, Albrecht



Abstract

Microcrystalline triacetylcellulose (dp = 10–20 μm) was used for analytical liquid chromatography at pressures around 50 bar. 1,3,5-Tri-tert.-butylbenzene is proposed as a compound which is not retained on this sorbent. Thus, reliable information about porosity, linear flow-rates, u, and relative retentions become available for the first time. An attempt was made to obtain the plate height, H, ...

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