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Automated apparatus for the rapid determination of liquid-liquid and solid-liquid phase transitions

Schrödle, S. ; Buchner, Richard ; Kunz, Werner



Abstract

An automated apparatus developed for the determination of liquid-liquid and solid-liquid equilibrium temperatures with a resolution of 1 mK and a traceable accuracy of 0.01 K is described. The amount of light transmitted through six sample cells placed in a computer controlled thermostat is recorded at heating or cooling rates from 0.075 to 15 K h(-1). The construction does not require expensive ...

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