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Cyclopentadiene Annelated [2.2]Paracylophanes: Novel Ligands Toward Multilayered Metal Complexes

Buchholz, Herwig ; Reiser, Oliver ; Meijere, Armin de


Pauson-Khand reactions of [2.2]paracyclophane-1,9-diene (2) and [2.2]paracyclophan-1-ene (3) with various acetylenes and octacarbonyldicobalt lead to monocyclopentenone anellated derivatives 5/6 and biscyclopentenone anellated derivative synanti-7 which can be converted to cyclopentadiene anellated systems 10/11 and 13. Their deprotonation with methyllithium yields cyclopentadienyl anions, ...


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