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Na3SbS3: Single Crystal X-ray Diffraction, Raman Spectroscopy, and Impedance Measurements

URN to cite this document:
urn:nbn:de:bvb:355-epub-278277
Pompe, Constantin ; Pfitzner, Arno
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Date of publication of this fulltext: 07 Mar 2013 12:50


Abstract

Na3SbS3 was prepared by the reaction of anhydrous Na2S, antimony, and sulfur in a ratio of 3:2:3 at 870 K. The pale yellow compound is air and moisture sensitive. A microcrystalline sample was obtained after annealing Na3SbS3 for two weeks at 720 K. The crystal structure of Na3SbS3 was determined by single-crystal X-ray diffraction at 123 K. Na3SbS3 crystallizes in the cubic space group P213 (No. ...

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