Na3SbS3: Single Crystal X-ray Diffraction, Raman Spectroscopy, and Impedance Measurements

URN to cite this document:: urn:nbn:de:bvb:355-epub-278277
DOI to cite this document:: 10.5283/epub.27827

Pompe, Constantin ; Pfitzner, Arno

Preview

PDF
(831kB)

Date of publication of this fulltext: 07 Mar 2013 12:50

Alternative links to fulltext:DOI

Details

Preview

Export bibliographical data

Abstract

Na3SbS3 was prepared by the reaction of anhydrous Na2S, antimony, and sulfur in a ratio of 3:2:3 at 870 K. The pale yellow compound is air and moisture sensitive. A microcrystalline sample was obtained after annealing Na3SbS3 for two weeks at 720 K. The crystal structure of Na3SbS3 was determined by single-crystal X-ray diffraction at 123 K. Na3SbS3 crystallizes in the cubic space group P213 (No. ...