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Wastl, Daniel S. ; Weymouth, Alfred J. ; Giessibl, Franz J.

Optimizing atomic resolution of force microscopy in ambient conditions

Article

Wastl, Daniel S. , Weymouth, Alfred J. and Giessibl, Franz J. (2013) Optimizing atomic resolution of force microscopy in ambient conditions. Physical Review B (PRB) 87 (24), 245415-1-245415-10.

DOI to cite this document: 10.5283/epub.28393


Abstract

Ambient operation poses a challenge to atomic force microscopy because in contrast to operation in vacuum or liquid environments, the cantilever dynamics change dramatically from oscillating in air to oscillating in a hydration layer when probing the sample. We demonstrate atomic resolution by imaging of the KBr(001) surface in ambient conditions by frequency-modulation atomic force microscopy ...

Ambient operation poses a challenge to atomic force microscopy because in contrast to operation in vacuum or liquid environments, the cantilever dynamics change dramatically from oscillating in air to oscillating in a hydration layer when probing the sample. We demonstrate atomic resolution by imaging of the KBr(001) surface in ambient conditions by frequency-modulation atomic force microscopy with a cantilever based on a quartz tuning fork (qPlus sensor) and analyze both long- and short-range contributions to the damping. The thickness of the hydration layer increases with relative humidity; thus varying humidity enables us to study the influence of the hydration layer thickness on cantilever damping. Starting with measurements of damping versus amplitude, we analyzed the signal and the noise characteristics at the atomic scale. We then determined the optimal amplitude which enabled us to acquire high-quality atomically resolved images.



Involved Institutions


Details

Item typeArticle
Journal or Publication TitlePhysical Review B (PRB)
PublisherAMER PHYSICAL SOC
Open Access TypeDue to SHERPA/RoMEO
Place of PublicationCOLLEGE PK
Volume87
Number of Issue or Book Chapter24
Page Range245415-1-245415-10
Date12 June 2013
Date of publication21 Jun 2013 06:07
InstitutionsPhysics > Institute of Experimental and Applied Physics > Chair Professor Giessibl > Group Franz J. Giessibl
Identification Number
ValueType
10.1103/PhysRevB.87.245415DOI
1303.5204v2arXiv ID
Classification
NotationType
07.79.LhPACS
34.20.-bPACS
68.08.-pPACS
68.37.PsPACS
KeywordsALKALI-HALIDE SURFACES; QUARTZ TUNING FORK; NACL(100) SURFACE; WATER-ADSORPTION; HYDRATION FORCES; CANTILEVERS; SENSOR; MODE; LIQUID; VACUUM;
Dewey Decimal Classification500 Science > 530 Physics
500 Science > 530 Physics
500 Science > 540 Chemistry & allied sciences
500 Science > 570 Life sciences
600 Technology > 600 Technology (Applied sciences)
600 Technology > 610 Medical sciences Medicine
StatusPublished
RefereedYes, this version has been refereed
Created at the University of RegensburgYes
URN of the UB Regensburgurn:nbn:de:bvb:355-epub-283932
Item ID28393

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