LiSbS2-mC16: Structure Determination from X-ray Powder Diffraction Data

URN to cite this document:: urn:nbn:de:bvb:355-epub-304075
DOI to cite this document:: 10.5283/epub.30407

Huber, Sebastian ; Pfitzner, Arno

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Date of publication of this fulltext: 11 Jul 2014 07:22

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Abstract

Monoclinic LiSbS2-mC(16) was synthesized by solid-state reaction of Li2S, Sb, and S in the ratio 1: 2: 5 at a temperature of 900 degrees C. The excess of sulfur serves as a kind of flux and is not incorporated in the structure. The product is air and moisture sensitive. The crystal structure of the dark red product was determined from X-ray powder diffraction data at 293 K. LiSbS2-mC(16) ...