Li17Sb13S28: A New Lithium Ion Conductor and addition to the Phase Diagram Li2S–Sb2S3

URN to cite this document:: urn:nbn:de:bvb:355-epub-324578
DOI to cite this document:: 10.5283/epub.32457

Huber, Sebastian ; Pfitzner, Arno

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Date of publication of this fulltext: 21 Sep 2015 14:02

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Abstract

Li17Sb13S28 was synthesized by solid-state reaction of stoichiometric amounts of anhydrous Li2S and Sb2S3. The crystal structure of Li17Sb13S28 was determined from dark-red single crystals at room temperature. The title compound crystallizes in the monoclinic space group C2/m (no. 12) with a=12.765(2) Å, b=11.6195(8) Å, c=9.2564(9) Å, β=119.665(6)°, V=1193.0(2) Å3, and Z=4 (data at 20 °C, lattice ...