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Iron-catalyzed olefin hydrogenation at 1 bar H2 with a FeCl3–LiAlH4 catalyst

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Gieshoff, Tim N. ; Villa, Matteo ; Welther, Alice ; Plois, Markus ; Chakraborty, Uttam ; Wolf, Robert ; Jacobi von Wangelin, Axel
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Date of publication of this fulltext: 12 Feb 2016 11:04


The scope and mechanism of a practical protocol for the iron-catalyzed hydrogenation of alkenes and alkynes at 1 bar H2 pressure were studied. The catalyst is formed from cheap chemicals (5 mol% FeCl3–LiAlH4, THF). A homogeneous mechanism operates at early stages of the reaction while active nanoparticles form upon ageing of the catalyst solution.

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