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GC analysis of trichloroacetic acid in water samples by large-volume injection and thermal decarboxylation in a programmed-temperature vaporizer

Drechsel, D. ; Dettmer, Katja ; Engewald, W. ; Bittner, T. ; Efner, J.


AGC method has been developed for the analysis of tricholoroacetic acid (TCA) in water samples. It entails large-volume injection (LVI) and programmed-temperature vaporization (PTV) of water samples, thermal decarboxylation of TCA to chloroform in the injector, and GC-ECD analysis of the decarboxylation product. Conditions such as final injector temperature, splitless time, and injection volume ...


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