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Nitrosonium-Mediated Phenol–Arene Cross-Coupling Involving Direct C–H Activation

Eisenhofer, Anna ; Wille, Uta ; König, Burkhard



Abstract

The nitrosonium ion (NO+) is a highly versatile nitration and nitrosation reagent, as well as a strong one-electron oxidant. Herein, we describe an environmentally benign and mild method for the in situ formation of NO+ from readily available inorganic nitrate salts, i.e. lithium nitrate, through a finely tuned interplay between formic acid and MeOH, which are used as the solvent system. This ...

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