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Systematic Evaluation of Non-Uniform Sampling Parameters in the Targeted Analysis of Urine Metabolites by1H,1H 2D NMR Spectroscopy

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von Schlippenbach, Trixi ; Oefner, Peter J. ; Gronwald, Wolfram
Date of publication of this fulltext: 28 Mar 2018 07:23


Non-uniform sampling (NUS) allows the accelerated acquisition of multidimensional NMR spectra. The aim of this contribution was the systematic evaluation of the impact of various quantitative NUS parameters on the accuracy and precision of 2D NMR measurements of urinary metabolites. Urine aliquots spiked with varying concentrations (15.6-500.0 mu M) of tryptophan, tyrosine, glutamine, glutamic ...


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