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Mo2 B4 O9 -Connecting Borate and Metal-Cluster Chemistry

Schmitt, Martin K. ; Janka, Oliver ; Pöttgen, Rainer ; Benndorf, Christopher ; de Oliveira, Marcos ; Eckert, Hellmut ; Pielnhofer, Florian ; Tragl, Amadeus-Samuel ; Weihrich, Richard ; Joachim, Bastian ; Johrendt, Dirk ; Huppertz, Hubert


We report on the first thoroughly characterized molybdenum borate, which was synthesized in a high-pressure/high-temperature experiment at 12.3 GPa/1300 degrees C using a Walker-type multianvil apparatus. Mo2B4O9 incorporates tetrahedral molybdenum clusters into an anionic borate crystal structure-a structural motif that has never been observed before in the wide field of borate crystal ...


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