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Synthesis and Molecular Structures of [Rh(η5 -C5 H5 )(coe)2 ] (coe = cis -cyclooctene) and [Rh(η5 -C5 H5 )(cod)] (cod = cis ,cis -η4 -1,5-cyclooctadiene)

Graf, Marion ; Böttcher, Hans-Christian ; Mayer, Peter ; Scheer, Manfred



Abstract

The synthesis and structural characterization of the new olefinic complex [Rh(eta(5)-C5H5)(coe)(2)] (2) (coe = cis-cyclooctene) is reported. The title compound could easily be prepared in good yield by reaction of [{Rh(mu-Cl)(coe)(2)}(2)] (1) with an appropriate amount of thallium cyclopentadienide in THF at room temperature. Single crystals of 2 were grown from n-hexane and were analyzed by ...

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