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[3+2] Fragmentation of a Pentaphosphido Ligand by Cyanide

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Hoidn, Christian M. ; Maier, Thomas M. ; Trabitsch, Karolina ; Wolf, Robert
License: Creative Commons Attribution Non-commercial 4.0
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Date of publication of this fulltext: 26 Feb 2020 14:47

This publication is part of the DEAL contract with Wiley.


The activation of white phosphorus (P4) by transition‐metal complexes has been studied for several decades, but the functionalization and release of the resulting (organo)phosphorus ligands has rarely been achieved. Herein we describe the formation of rare diphosphan‐1‐ide anions from a P5 ligand by treatment with cyanide. Cobalt diorganopentaphosphido complexes have been synthesized by a ...


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