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Stabilization of Pentaphospholes as η5 -coordinating Ligands. Stabilisierung von Pentaphospholen als η5-koordinierende Liganden

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Riesinger, Christoph ; Balazs, Gabor ; Bodensteiner, Michael ; Scheer, Manfred
License: Creative Commons: Attribution-Noncommercial-No Derivative Works 3.0
PDF - Published Version
in: Internat. Edition
License: Creative Commons Attribution Non-commercial No Derivatives 4.0
PDF - Published Version
in: dtsch. Ausgabe
Date of publication of this fulltext: 25 Jan 2021 06:38

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Electrophilic functionalisation of [Cp*Fe(eta(5)-P-5)] (1) yields the first transition-metal complexes of pentaphospholes (cyclo-P5R). Silylation of1with [(Et3Si)(2)(mu-H)][B(C6F5)(4)] leads to the ionic species [Cp*Fe(eta(5)-P5SiEt3)][B(C6F5)(4)] (2), whose subsequent reaction with H2O yields the parent compound [Cp*Fe(eta(5)-P5H)][B(C6F5)(4)] (3). The synthesis of a carbon-substituted ...


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