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Low-Valence Anionic α-Diimine Iron Complexes: Synthesis, Characterization, and Catalytic Hydroboration Studies

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Maier, Thomas M. ; Gawron, Martin ; Coburger, Peter ; Bodensteiner, Michael ; Wolf, Robert ; van Leest, Nicolaas P. ; de Bruin, Bas ; Demeshko, Serhiy ; Meyer, Franc
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Date of publication of this fulltext: 18 May 2021 07:03


The synthesis of rare anionic heteroleptic and homoleptic alpha-diimine iron complexes is described. Heteroleptic BIAN (bis(aryl)iminoacenaphthene) complexes 1-[K([18]c-6)-(thf)(0.5)] and 2-[K([18]c-6)(thf)(2)] were synthesized by reduction of the [(BIAN)FeBr2] precursor complex using stoichiometric amounts of potassium graphite in the presence of the corresponding olefin. The electronic ...


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