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Synthesis and Characterization of Three New Lithium-Scandium Hexathiohypodiphosphates: Li4-3xScxP2S6(x= 0.358),m-LiScP2S6, andt-LiScP2S6

Schoop, Leslie Mareike ; Eger, Roland ; Pielnhofer, Florian ; Schneider, Christian ; Nuss, Jürgen ; Lotsch, Bettina Valeska


We report the first examples of lithium rare earth metal hexathiohypodiphosphates(IV). Three new lithium-scandium hexathiohypodiphosphates(IV) were synthesized and characterized. The compounds crystallize in three different structure types, featuring isolated ethane-like [P2S6](4-) hexathiohypodiphosphate(IV) units. Li2.926Sc0.358P2S6 or Li4-3xScxP2S6 (x = 0.358) crystallizes in the space group ...


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