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Visible Light-Mediated Decarboxylation Rearrangement Cascade of ω-Aryl-N-(acyloxy)phthalimides

Faderl, Christian ; Budde, Simon ; Kachkovskyi, Georgiy ; Rackl, Daniel ; Reiser, Oliver


A Smiles-type radical rearrangement induced by visible-light-mediated decarboxylation of omega-aryl-N-(acyloxy)phthalimides was developed, giving rise to pharmacologically important substance classes: phenylethylamine derivatives, dihydroisoquinolinones, and benzoazepinones were synthesized on the basis of readily available benzoic acids or benzaldehydes and beta- or gamma-amino acids. This ...


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