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Open Chain Polyarsenides of the Lanthanides

Schoo, Christoph ; Köppe, Ralf ; Piesch, Martin ; Gamer, Michael T. ; Konchenko, Sergey N. ; Scheer, Manfred ; Roesky, Peter W.


The reaction of [(Cp'''Co)(2)(mu, eta(2:2)-As-2)(2)] with the decamethylsamarocenes [Cp*Sm-2(THF)(2)] or [Cp*Sm-2], or the bis(tetramethyl-n-propyl) samarocene [(C5Me4(n-propyl))(2)Sm] resulted in the mixed d/f polyarsenides [(Cp'''Co)(2)As4Sm(h(5)C(5)Me(4)R) (2)] (R=Me, n-propyl). They are the first structural representatives of open chain- like polyarsenides as ligands in the coordination ...


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