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The very first normal-pressure tin borate Sn3B4O9, and the intermediate Sn2[B7O12]F

Schäfer, Martin J. ; Jantz, Stephan G. ; Pielnhofer, Florian ; Höppe, Henning A.


Aside from amorphous phases, only a single crystalline tin borate had been synthesised so far under high pressure. In this work, we present the very first crystalline ternary tin borate Sn3B4O9 synthesised under ambient pressure by decomposition of Sn-3[B3O7]F above 500 degrees C. The crystal structure of Sn3B4O9 (P2(1)/c, Z = 4, a = 768.07(3) pm, b = 1206.78(4) pm, c = 924.96(3) pm, beta = ...


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