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Syntheses and Structures of Transition Metal Complexes with Phosphanylphosphinidene Chalcogenide Ligands

Ordyszewska, Anna ; Szynkiewicz, Natalia ; Ponikiewski, Łukasz ; Scheer, Manfred ; Pikies, Jerzy ; Grubba, Rafał


The reactivity of the phosphanylphosphinidene complex [(DippN)(2)W(Cl)(eta(2)-P-PtBu2)](-) (1) toward chalcogens (Ch = Se, S) was studied. Reactions of stoichiometric amounts of 1 with chalcogens in DME yielded monomeric tungsten complexes with phosphanylphosphinidene chalcogenide ligands of the formula tBu(2)P-P-Ch (Ch = Se (in 2) and S (in 5)), which can be regarded as products of the addition ...


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