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Photocatalytic Arylation of P4 and PH3: Reaction Development Through Mechanistic Insight

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Rothfelder, Robin ; Streitferdt, Verena ; Lennert, Ulrich ; Cammarata, Jose ; Scott, Daniel J. ; Zeitler, Kirsten ; Gschwind, Ruth M. ; Wolf, Robert
Date of publication of this fulltext: 14 Oct 2021 05:48

This publication is part of the DEAL contract with Wiley.


Detailed P-31{H-1} NMR spectroscopic investigations provide deeper insight into the complex, multi-step mechanisms involved in the recently reported photocatalytic arylation of white phosphorus (P-4). Specifically, these studies have identified a number of previously unrecognized side products, which arise from an unexpected non-innocent behavior of the commonly employed terminal reductant Et3N. ...


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