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Synthesis‐Controlled Polymorphism and Optical Properties of Phyllosilicate‐Analogous Borosulfates M [B 2 (SO 4 ) 4 ] ( M =Mg, Co)

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Netzsch, Philip ; Pielnhofer, Florian ; Glaum, Robert ; Höppe, Henning A.
Date of publication of this fulltext: 11 Oct 2021 12:41


Increased synthetic control in borosulfate chemistry leads to the access of various new compounds. Herein, the polymorphism of phyllosilicate-analogous borosulfates is unraveled by adjusting the oleum (65 % SO3) content. The new polymorphs beta-Mg[B-2(SO4)(4)] and alpha-Co[B-2(SO4)(4)] both consist of similar layers of alternating borate and sulfate tetrahedra, but differ in the position of ...


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