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Selectivity control in thiol–yne click reactions via visible light induced associative electron upconversion

Burykina, Julia V. ; Shlapakov, Nikita S. ; Gordeev, Evgeniy G. ; König, Burkhard ; Ananikov, Valentine P.


An associative electron upconversion is proposed as a key step determining the selectivity of thiol-yne coupling. The developed synthetic approach provided an efficient tool to access a comprehensive range of products - four types of vinyl sulfides were prepared in high yields and selectivity. We report practically important transition-metal-free regioselective thiol-yne addition and formation of ...


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