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Halogenation of the Hexaphosphabenzene Complex [(Cp*Mo) 2 (μ,η 6 :η 6 ‐P 6 )]: Snapshots on the Reaction Progress

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Garbagnati, Anna ; Seidl, Michael ; Balázs, Gábor ; Scheer, Manfred
Date of publication of this fulltext: 14 Jun 2022 08:33

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The oxidation of [(Cp*Mo)(2)(mu,eta(6):eta(6)-P-6)] (1) with halogens or halogen sources was investigated. The iodination afforded the ionic complexes [(Cp*Mo)(2)(mu,eta(3):eta(3)-P-3)(mu,eta(1):eta(1):eta(1):eta(1)-P3I3)][X] (X=I-3(-), I-) (2) and [(Cp*Mo)(2)(mu,eta(4):eta(4)-P-4)(mu-PI2)][I-3] (3), while the reaction with PBr5 led to the complexes ...


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