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Synthesis and Redox Chemistry of a Homoleptic Iron Arsenic Prismane Cluster

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Riesinger, Christoph ; Dütsch, Luis ; Scheer, Manfred
Date of publication of this fulltext: 06 Sep 2022 05:40


The redox chemistry of the homoleptic iron prismane cluster [{Cp*Fe}3(μ3,η4:4:4-As6)] (A, Cp*=C5Me5) is investigated both electrochemically and synthetically. While its first oxidation leads to the diamagnetic species [{Cp*Fe}3(μ3,η4:4:4-As6)][X] ([1][TEF], [1][FAl], [TEF]−=[Al{OC(CF3)3}4]−, [FAl]−=[FAl{O(1-C6F5)C6F10}3]−), the second oxidation yields the paramagnetic ...


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