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Synthesis of Unprecedented 4d/4f‐Polypnictogens

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Reinfandt, Niklas ; Schoo, Christoph ; Dütsch, Luis ; Köppe, Ralf ; Konchenko, Sergey N. ; Scheer, Manfred ; Roesky, Peter W.
Date of publication of this fulltext: 29 Feb 2024 12:27


A series of 4d/4f-polyarsenides, -polyarsines and -polystibines was obtained by reduction of the Mo-pnictide precursor complexes [{(CpMo)-Mo-t(CO)(2)}(2)(mu,eta(2:2)-E-2)] (E=As, Sb; Cp-t=tBu substituted cyclopentadienyl) with two different divalent samarocenes [Cp*Sm-2] and [(Cp-Me4nPr)(2)Sm]. For the reductive conversion of the Mo-stibide only one product was isolated, featuring a planar ...


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