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Synthesis and Structure of a Stabilized 10-Membered Cyclic Enediyne

Pitsch, W. ; Klein, M. ; Zabel, M. ; König, B.


The synthesis and structure of an acetal protected 10-membered cyclic enediyne-1,2-diol rac-10 is reported. The conformational constrain of the unsaturated macrocycle by the acetal protection group prevents the thermal cyclization reaction of the endiyne during synthesis and purification.

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