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Tetrahydrofuran Cα-Tetrasubstituted Amino Acids: Two Consecutive β Turns in a Crystalline Linear Tripeptide

Maity, P. ; Zabel, M. ; König, B.



Abstract

The synthesis of tetrahydrofuran Cα-tetrasubstituted amino acids (TAAs) and their effect on the conformation in small peptides are reported. The synthesis starts from the protein amino acid methionine, which is protected at the C and N terminus and converted into the corresponding sulfonium salt by alkylation. Simple base treatment in the presence of an aryl aldehyde leads to the formation of ...

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