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Pyramidal Stability of Chiral-at-Metal Half-Sandwich 16-Electron Fragments [CpRu(P−P′)]

Brunner, Henri ; Muschiol, Manfred ; Tsuno, Takashi ; Takahashi, Takemoto ; Zabel, Manfred



Zusammenfassung

The chiral-at-metal diastereomers (R-Ru,R-C)- and (S-Ru,R-C)-[CpRu(P-P')Hal] (P-P' = (R)-Prophos and (R,R)-Norphos, Hal = Cl, Br, and I) were synthesized, separated, and characterized by X-ray crystallography. Halide exchange and epimerization reactions were studied in 9:1 and 1:1 chloroform/methanol mixtures proceeding at room temperature or slightly above according to first-order. The ...

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